http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113105493-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F7-083 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F7-0816 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F7-0807 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F7-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F7-08 |
filingDate | 2021-03-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-03-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2022-03-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-113105493-B |
titleOfInvention | Naphthosilole compound and synthesis method for preparing naphthosilole compound through photocatalysis |
abstract | The invention discloses a naphthosilole compound and a synthetic method for preparing the naphthosilole compound by photocatalysis; the general formula of the structure is shown as C, and the method comprises the following steps: mixing o-alkynyl aryl vinyl silane, aryl sulfonyl azide, a photocatalyst and alkali, adding an organic solvent, irradiating the mixture by blue light, reacting at 60-80 ℃, cooling to room temperature after the reaction is finished, spin-drying the solvent in vacuum, and carrying out column chromatography to obtain the naphthosilole compound. The method has the advantages of simple and easy operation process, simple and convenient steps and easy purification of the product. |
priorityDate | 2021-03-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 66.