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publicationDate 2021-07-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113104892-A
titleOfInvention A method for preparing large-size ultra-thin molybdenum disulfide nanosheets by chemical intercalation-assisted liquid phase exfoliation and the prepared product thereof
abstract The invention discloses a method for preparing large-sized ultra-thin molybdenum disulfide nanosheets by chemical intercalation-assisted liquid phase exfoliation and a prepared product thereof. The molybdenum disulfide nanosheets prepared by the method of the present invention are single-layer or few-layered, the thickness of the nanosheets is 0.8-2.5 nm, and the diameter of the sheets is 0.5-10 μm. The specific steps of the preparation method are as follows: 1. Mix molybdenum disulfide powder with an alkali metal pyrene reagent, react for 0.5-6 h, and after the reaction ends, perform suction filtration to obtain an intercalated compound of alkali metal ion intercalation. 2. Immediately disperse the intercalating compound of the above-mentioned alkali metal ion intercalation in a solvent, and ultrasonically peel for 15-30 min, to obtain the large-sized ultra-thin molybdenum disulfide nanosheets. The invention has simple process and low cost, and can realize high-efficiency preparation of high-quality ultra-thin molybdenum disulfide nanosheets.
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