http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113072439-A

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C50-34
filingDate 2021-03-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_187fc937562b14d79f50bcad316c3695
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9e11d8dbf9e3b25d7aed4997b6f3fd9c
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publicationDate 2021-07-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113072439-A
titleOfInvention A cleaning process for synthesizing 1,4-dihydroxyanthraquinone
abstract The invention relates to the technical field of dye intermediates, in particular to a cleaning process for synthesizing 1,4-dihydroxyanthraquinone, comprising the following steps: sequentially adding metered proportions of 98% sulfuric acid, boric anhydride, phthalic anhydride and Hydroquinone, stir evenly and then heat up to 100~180°C, and keep the reaction for 2~24h; after the insulation reaction is over, cool down the material and transfer it to another reaction vessel for hydrolysis; after the hydrolysis is completed, cool down, filter and wash with water to obtain 1 , 4-dihydroxyanthraquinone. The cleaning process for synthesizing 1,4-dihydroxyanthraquinone provided by the invention can reduce the consumption of raw material phthalic anhydride, greatly reduce the difficulty of wastewater treatment, and also reduce the production cost; rate has also improved.
priorityDate 2021-03-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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Total number of triples: 46.