http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113003613-A

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publicationDate 2021-06-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113003613-A
titleOfInvention A kind of preparation method of 2-4μm battery grade cobalt tetroxide
abstract The invention discloses a preparation method of 2-4 μm battery-grade cobalt tetroxide. The method comprises the following steps: 1) adding cobalt salt solution and liquid caustic soda into a reactor containing bottom liquid and passing air in parallel, and The pH value of the system is controlled by adjusting the flow rate of the liquid caustic soda and the co-precipitation reaction is carried out at a certain stirring rate. After the reaction liquid starts to overflow, the pH value of the reaction system is decreased by 0.1 and the flow rate of the cobalt salt is increased by 20L/h every hour. Until the pH value of the reaction system drops to 9.5 and the cobalt salt flow rate increases to 340L/h, the particle size is continuously monitored to obtain cobalt oxyhydroxide slurry; 2) the cobalt oxyhydroxide slurry is sequentially aged and dried to obtain the dried cobalt oxyhydroxide slurry. cobalt oxyhydroxide; 3) calcining the dried cobalt oxyhydroxide to obtain battery grade cobalt tetraoxide. By adopting the method of the present invention, the tap density of the obtained battery-grade cobalt tetroxide will be much higher than the tap density of the cobalt tetroxide with the same particle size and specification obtained in the prior art.
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priorityDate 2019-12-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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