http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112921346-B
Outgoing Links
Predicate | Object |
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classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-584 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C25B3-09 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C25B3-07 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C25B3-23 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C25B3-05 |
filingDate | 2021-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-07-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2022-07-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-112921346-B |
titleOfInvention | A kind of electrochemical synthesis method of 3-formyl indole derivatives |
abstract | The invention discloses an electrochemical synthesis method of 3-formyl indole derivatives. The method of the invention is as follows: using a non-separated electrolytic cell as a reaction vessel, adding N,N,N',N'-tetramethylethylenediamine, electrolyte, water and organic solvent into it, stirring uniformly to form a reaction solution, and then adding The positive electrode and the negative electrode of the electrode are respectively inserted into the reaction solution, and the constant current is turned on to stir the reaction. After the reaction is completed, the 3-formyl indole derivative is obtained by separation by column chromatography, and the drug depigmentation can be further prepared. The method of the invention does not need to use metal catalysts and oxidants, only electrocatalytic oxidation is used, and the method has the characteristics of easy availability of raw materials, simple operation, applicable electrolytes and solvents, and the like, and has great practical value and social and economic benefits. |
priorityDate | 2021-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 84.