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filingDate 2020-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-112831800-B
titleOfInvention Preparation method of molybdenum-based composite material electrode plate
abstract The invention relates to a preparation method of a molybdenum-based composite electrode plate, which comprises the steps of pouring molybdenum powder and nickel powder into excessive titanium tetrachloride in a glove box filled with argon, fully stirring and filtering, placing mixed powder adhered with the titanium tetrachloride in a quartz tube of a tube furnace, introducing oxygen for heat treatment, placing the mixed powder after the heat treatment in a graphite mold for discharge plasma sintering, soaking a sintered sample in the titanium tetrachloride again, taking out the sample after filtering, placing the sample in the quartz tube of the tube furnace again, sequentially introducing the oxygen and hydrogen sulfide for heat treatment, and obtaining the molybdenum-based composite electrode plate after the heat treatment. The invention has low cost, convenient operation and controllable process. The obtained electrode plate has high catalytic activity, good conductivity, certain mechanical property and machinability, can be used as a catalyst, a current collector and an electrode to catalyze water decomposition, and has wide industrial production prospect.
priorityDate 2020-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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