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filingDate 2020-12-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-11-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-11-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-112745407-B
titleOfInvention A kind of preparation method and application of polyvinyl acetal resin
abstract The invention discloses a preparation method of polyvinyl acetal resin and its application. The preparation method of polyvinyl acetal comprises the following steps: S10, dissolving polyvinyl alcohol and an acidic catalyst in pure water, and fully stirring to form a mixed solution , cooling the mixed solution to below 20°C; S20, adding polyvinyl acetal raw materials, emulsifiers and aldehydes to the cooled mixed solution, and stirring at 30-70°C for 1.5-5 hours to obtain a mixed solution A; S30, Add sodium hydroxide solution to the mixed solution A to terminate the reaction and obtain a suspension containing solids; S40, remove impurities in the suspension, then separate the suspension from solid and liquid, and wash and dry the obtained solids, namely The polyvinyl acetal resin can be obtained; wherein, the ratio of meso and racemic acetal isomers in the polyvinyl acetal raw material is 3.5-15. By adding high m/r polyvinyl acetal raw materials to the reaction at the low temperature stage, a polyvinyl acetal resin with an acetalization degree of 78% or more and an m/r of 3.5 or more is prepared.
priorityDate 2020-12-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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