http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112625249-A

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filingDate 2020-11-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5eb64340b3e4b0235b97434c803067a9
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publicationDate 2021-04-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-112625249-A
titleOfInvention A new type of phosphorus, nitrogen and sulfur flame retardant and preparation method thereof
abstract The invention discloses a novel phosphorus-nitrogen-sulfur flame retardant and a preparation method thereof. In the reaction device, phosphorus oxychloride and thiomorpholine are mixed in a molar ratio of 1:1, and the reaction temperature is 0-10°C to obtain a chlorophosphoramide compound. The chlorophosphoramide compound is hydrolyzed to obtain the thiomorpholine phosphoramide compound. After the thiomorpholine phosphoric acid amide and 1%-5% amino trimethylene phosphonic acid are fully mixed, the novel phosphorus nitrogen sulfur flame retardant is prepared by dehydration reaction in an inert atmosphere or a high boiling point solvent, and the reaction temperature is 250 ℃ ‑320°C.
priorityDate 2020-11-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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