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filingDate 2020-12-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2021-04-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-112592491-A
titleOfInvention A kind of preparation method of metal organic framework based on ionic liquid microemulsion
abstract The invention discloses a method for preparing a metal-organic framework based on ionic liquid microemulsion. ) adding an organic ligand into the microemulsion, mixing and stirring to obtain a mixed solution A; step 3) adding a transition metal salt to the microemulsion, mixing and stirring to obtain a mixed solution B; step 4) mixing the mixed solution A and mixed solution B are mixed and stirred, reacted at a preset temperature for a preset time, centrifuged to obtain a solid reactant, and washed with a mixed solution of dichloromethane and ethanol to obtain a metal organic framework. The preparation method of the invention can control and synthesize metal-organic framework crystals with different morphologies, different sizes and different metal centers by adjusting the alkyl chain length of the ionic liquid in the microemulsion, the type of oil phase and the proportion of each component.
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