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filingDate 2020-12-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-09-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-112536039-B
titleOfInvention Preparation method of visible light catalytic material of composite oxide with hierarchical structure
abstract The invention relates to preparation of a semiconductor material, and aims to provide a preparation method of a visible light catalytic material of a composite oxide with a hierarchical structure. The method comprises the following steps: dissolving copper salt and bismuth salt in urea aqueous solution, and uniformly mixing to obtain a blue-white precursor solution; dropwise adding a sodium hydroxide solution into the precursor solution to obtain a dark green precursor suspension; and cooling after hydrothermal reaction, and centrifuging and drying the brownish black precipitate to obtain the visible light catalytic material. The microsphere obtained by the invention is formed by self-assembling nano rods, has smaller diameter and larger specific surface area of the material, can provide more reaction sites for photocatalytic reaction, and is beneficial to improving the photocatalytic reaction efficiency. The method utilizes the decomposition reaction of urea in the hydrothermal reaction process, and the generated gas molecules form internal stress in the sphere to loosen the microsphere and increase the specific surface area of the material. Meanwhile, micropores are formed on the surface of the material in the escape process of gas molecules, so that the separation of photon-generated carriers is promoted, and the photocatalytic reaction efficiency is improved.
priorityDate 2020-12-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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