http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112457494-A

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filingDate 2020-12-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5377307b4b71cb163ef9924d842741b2
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publicationDate 2021-03-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-112457494-A
titleOfInvention A kind of liquid crystal optical film production method
abstract The invention relates to a method for manufacturing a liquid crystal optical film, comprising: synthesis of 3,3'-dimethyl-4,4'-diaminodiphenylmethane, synthesis of 4,4'-diaminodiphenylpiperazine, 4 , the synthesis of 4'-diaminobenzoylpiperazine, the preparation of sample 1, the preparation of sample 2, the preparation of sample 3, the preparation of sample 4, the preparation of film; it is characterized in that: the 3,3'-di Synthesis of methyl-4,4'-diaminodiphenylmethane: install a thermometer, a condenser and a stirrer respectively on a 500ml three-necked flask, then add 0.5mol hydrochloric acid, 100ml water, and 0.5mol o-toluidine for stirring and cooling together to 15°C, and then dropwise add 0.25mol 40% formaldehyde solution to the mixed solution, fully stirring during the dropping process, and pay attention to the reaction temperature; the present invention has good transparency, solubility, The mechanical properties, heat resistance and negative birefringence are low in cost and have the advantages of compensating for the liquid crystal display, thus effectively solving the problems and deficiencies proposed by the present invention.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113488743-A
priorityDate 2020-12-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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