Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_f758dbe45d1c0efd81aed6ae49981b71 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d80228fea1bfe12324a6d4353d6702eb |
classificationCPCAdditional |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N2030-025 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N2030-067 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-7206 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-26 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-26 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-72 |
filingDate |
2019-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_51a408fd8d767f7dd2771fd7c1277a3e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b2d74f61572915f310ee19d6de23616a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0ea3ca778692aab177eb4bfe3419845f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_60ba0a788708e4ccec5ac41727a21b2b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3f5bfad9b1c52e5f5d9753af1f662ea4 |
publicationDate |
2021-03-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
CN-112444571-A |
titleOfInvention |
Method for the detection of organic compounds in titanium tetrachloride by large-volume headspace thermal desorption gas chromatography-mass spectrometry |
abstract |
The invention discloses a large-volume headspace-thermal desorption-gas chromatography-mass spectrometry combined detection method for organic matter in titanium tetrachloride. The invention includes the following steps: hydrolyzing titanium tetrachloride, putting it into a large-volume headspace sampler for heating, and simultaneously adsorbing organic matter in the headspace gas with an adsorption tube; after sampling, putting the adsorption tube into a thermal analyzer for analysis, and analyzing The outgoing substances are introduced into the GC-MS for testing, and the GC-MS data is analyzed to determine the organic impurities in titanium tetrachloride. The invention has accurate qualitative and high sensitivity, and the detection limit can be as low as ng/kg level. Provide scientific and effective data for quality monitoring of titanium tetrachloride production and recycling, polyolefin catalyst research and development. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113082941-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114740118-A |
priorityDate |
2019-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |