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filingDate 2020-11-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-112358411-B
titleOfInvention Process and device for continuously producing m-aminoacetanilide hydrochloride
abstract The invention discloses a process and a system for continuously producing m-aminoacetanilide hydrochloride at high temperature and under pressure. The process comprises the following steps: mother liquor water, acetic acid, m-phenylenediamine and hydrogen chloride gas are continuously conveyed to a closed hypergravity reactor, materials in the hypergravity reactor are continuously discharged, part of the materials are returned to the hypergravity reactor for circulation after passing through a closed first heat exchanger, part of the materials enter a crystallization kettle and are treated by a separation device, m-aminoacetanilide hydrochloride finished products and mother liquor water are obtained, and the mother liquor water is collected and recycled. The system comprises a second heat exchanger, a closed hypergravity reactor, a closed first heat exchanger, a crystallization kettle, a separation device and a mother liquor water collection device which are connected in sequence; the second heat exchanger is used for preheating acetic acid and m-phenylenediamine; and a closed loop is formed between the hypergravity reactor and the first heat exchanger.
priorityDate 2020-11-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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