http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112341318-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_ed36fe37df6cc5bdbb474a254834741d |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C41-01 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C41-34 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-253 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-01 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-34 |
filingDate | 2019-08-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2b17fdf5707fc676b8baf54b4f6d5525 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7e8b4fc785bceb4a4146c30e80e1fd39 |
publicationDate | 2021-02-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-112341318-A |
titleOfInvention | A kind of method for preparing concentrated vanillin from sassafras oil |
abstract | The invention discloses a method for preparing concentrated vanillin from sassafras oil. The sassafras oil is used as a raw material, the amount of KOH and methanol is adjusted when the safrole is ring-opened and isomerized, and the ring-opening method is carried out by distilling methanol with water. , the reaction is milder and controllable, and the ring-opening product is not acidified, and then directly ethylated with diethyl sulfate, the reaction temperature is greatly reduced, the process is simple, and the yield is high; Phenol, synthesizing ethyl vanillin through oxidation reaction, not only reduces the treatment process and cost of the by-product, but also further reduces the cost of the by-product ethyl vanillin, which is an ideal industrialized preparation method Lansing's route. |
priorityDate | 2019-08-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 54.