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filingDate 2020-10-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-112233908-B
titleOfInvention Porous polyaniline composite electrode material doped with vanadium dioxide and preparation method thereof
abstract The invention belongs to the field of batteries, and particularly relates to a porous polyaniline composite electrode material doped with vanadium dioxide and a preparation method thereof. The invention aims to solve the technical problem of providing a preparation method of a porous polyaniline composite electrode material doped with vanadium dioxide, which comprises the following steps: A. uniformly mixing carbonate, nano vanadium dioxide, a solvent and aniline, then atomizing and adding an aqueous solution of ammonium persulfate and polyethylene glycol with the pH value of 0-4, and reacting to obtain an emulsion; B. b, uniformly mixing the emulsion obtained in the step A and aniline, and adjusting the pH of the system to 0-2; C. inserting a saturated calomel electrode, a platinum electrode and foamed nickel into the solution obtained in the step B, and carrying out constant-current electrochemical reaction to obtain a foamed nickel composite material; D. c, soaking the foamed nickel composite material obtained in the step C in water, then adding hydrazine hydrate, reacting at 80-95 ℃, and cooling to room temperature; E. taking out the materials, soaking, washing and drying. The electrode material obtained by the method has excellent performance.
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