| abstract |
The method relates to a method for synthesizing phosphoimide compounds, and belongs to the field of metal-catalyzed organic synthesis. A method for synthesizing phosphonimide compounds, comprising the following steps: adding N-hydrocarbonyloxyamide derivative, tertiary phosphine, catalyst, and organic solvent into a reaction vessel, reacting in an air atmosphere at room temperature, and finishing the reaction After post-treatment, phosphoimide compounds are obtained. The method for synthesizing phosphonimide compounds disclosed in the present invention has the following advantages: (1) wide range of substrates; (2) relatively low price of catalyst and less amount of catalyst; (3) simple reaction operation ; (4) The reaction yield is higher, and a higher yield can still be achieved by scaling up to a gram-level reaction. |