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filingDate 2020-07-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-111876999-B
titleOfInvention A kind of carbon nanotube-carbon fiber multi-scale reinforcement and its preparation method and application
abstract The invention discloses a process scheme for growing carbon nanotubes on the surface of continuous carbon fiber tows by catalytic chemical vapor deposition using a multi-component catalytic system containing copper components. The implementation method of the present invention includes the following steps: taking copper nitrate and ferric nitrate as necessary options, cobalt nitrate and nickel nitrate as optional options, configuring a catalyst precursor solution with anhydrous ethanol as a solvent, and then feeding the surface-activated carbon fibers into the solution dipping in an oven for 10-15 min and then drying in an oven; sending the carbon fiber bundles with catalyst precursors on the surface into a tube furnace, and performing catalyst reduction and CCVD growth of carbon nanotubes, respectively, to obtain carbon nanotube-carbon fiber multi-component Scale Enhancer. The invention can obtain the carbon nanotube-carbon fiber multi-scale reinforcement with more uniform distribution of carbon nanotubes and more regular arrangement of carbon atoms, and can significantly improve the interface bonding ability of the carbon fiber composite material.
priorityDate 2020-07-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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