http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111848377-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_ddbaea849acfed496cca3b796cf47858 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J23-888 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C45-41 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C47-575 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C45-41 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J23-888 |
filingDate | 2020-08-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_46c4e10c45cc08243b735f899dd31e53 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f939d0070ffea088ba671870326ae7b2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e35a198b9c1b608097d81099ef63cfd4 |
publicationDate | 2020-10-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-111848377-A |
titleOfInvention | The preparation method of ethyl vanillin |
abstract | The present invention relates to a preparation method of ethyl vanillin. The preparation method of the ethyl vanillin comprises the following steps: firstly preparing a copper oxide-tungsten oxide catalyst supported by an inorganic oxide, then 3-ethoxy-4-hydroxyglycolic acid, an inorganic oxide-supported catalyst The copper oxide-tungsten oxide catalyst and tetrahydrofuran were sequentially introduced into the reaction kettle, sealed, then purged with nitrogen, purged with oxygen, charged with oxygen to 0.5-1MPa, and then reacted at 80-90°C and 0.7-1.2MPa for 4- 6h. By adopting the method to prepare ethyl vanillin, the conversion rate of 3-ethoxy-4-hydroxyglycolic acid can reach over 99%, and the selectivity of ethyl vanillin can reach over 95%. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112973725-A |
priorityDate | 2020-08-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 59.