http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111825515-A

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C5-367
filingDate 2020-08-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0f77d5ed51427f016ebf5ac1e5b1bcec
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publicationDate 2020-10-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-111825515-A
titleOfInvention A kind of method for preparing p-cymene from dipentene
abstract The present invention relates to a method for preparing p-cymene from dipentene. The method includes the following steps: S1, continuously feeding nitrogen into the fixed-bed reactor; a catalyst bed is arranged in the fixed-bed reactor, and the catalyst bed is a θ ring packing loaded with a powdered catalyst; S2, Dipentene is vaporized at 180-220 ℃ to form steam, and the steam is passed into and filled with the fixed-bed reactor and then evacuated; the temperature in the fixed-bed reactor is 180-240 ℃, and the vacuum degree is 0.04-0.095MPa; the steam is continuously fed into the fixed-bed reactor to generate p-cymene by catalytic dehydrogenation reaction. The method can realize simple, efficient and continuous preparation of high-purity p-cymene, and the content of p-cymene is more than 92%.
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