http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111635322-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_2feb9b3a2ee1ee63f9d6e913f28356a9 |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J2219-0086 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C209-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J19-0093 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C209-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C211-52 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J19-00 |
filingDate | 2020-06-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_db8461b1edc40dc8c75524c993f94a8e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f9b35b5f603a68cfb1a932c6701de9a2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_afaf6489a034640a0771839a0f7c79ac http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7ed2305c436d192442802a44b6a4bd6e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_90c111354715edcea05fd21b4589429c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0e0179ae9d180855b04541528478f0ca http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6f173064127531bae29fcdcaeb7a8461 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b5a5e2eb620dbeaf144e9bf5e866ffd5 |
publicationDate | 2020-09-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-111635322-A |
titleOfInvention | A kind of method utilizing microreactor to prepare 2,4-dinitroaniline |
abstract | The invention relates to the technical field of preparation of 2,4-dinitroaniline, in particular to a method for preparing 2,4-dinitroaniline by using a microreactor. The steps are: (1) preparing equipment, preparing a preheater, The microreactor and two chromatographic pumps; (2) connect the reaction equipment, connect the two chromatographic pumps to the preheater and the microreactor respectively, and then connect the preheater to the microreactor, and connect the preheater to the microreactor after the connection is completed; The microreactor is placed in a constant temperature oil bath; (3) the transport of the reaction material, the ammonia water is transported to the preheater at a preset flow rate, and the melted 2,4-dinitrochlorobenzene is transported to the microreactor at a preset flow rate. Mixed reaction with ammonia water in the reactor to obtain 2,4-dinitroaniline; (4) according to step (3), after the material reaction is completed, excess ammonia is re-made into ammonia water for reuse by the ammonia recovery device, and the reaction is The ammonia generated by the reaction of the produced ammonium chloride and potassium hydroxide continues to be reused, and the invention has the characteristics of high production efficiency, low energy consumption, economical and environmental protection, safety and reliability. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114181089-A |
priorityDate | 2020-06-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 44.