http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111579673-B
Outgoing Links
Predicate | Object |
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classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N2030-062 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N2030-146 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B82Y15-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B82Y40-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-72 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B82Y40-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B82Y15-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-72 |
filingDate | 2020-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-07-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2022-07-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-111579673-B |
titleOfInvention | A kind of purification and detection method of fipronil and its metabolites in eggs |
abstract | The invention provides a purification and detection method for fipronil and its metabolites in eggs, and solves the purification and detection method for fipronil and its metabolites in eggs in the prior art, and the quantification limit is high, and the detection Insufficient sensitivity and low detection accuracy are technical problems. The purification and detection method includes the following steps: (1) preparing magnetic nanomaterials; (2) sample pretreatment; (3) using ultra-high performance liquid chromatography-Q-Exactive high-resolution mass spectrometry for detection and analysis. The detection limit and the quantification limit of the purification detection method of the present invention can reach 0.002-0.005 μg/kg and 0.006-0.015 μg/kg, and have the advantages of simple and rapid analysis, high sensitivity and precision, and good reproducibility , quantitative accuracy and high recovery rate, can accurately analyze the advantages of fipronil and its metabolites in eggs. |
priorityDate | 2020-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 65.