http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111517975-B

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C227-04
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C231-02
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C227-16
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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-02
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C237-30
filingDate 2020-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-12-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-12-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-111517975-B
titleOfInvention A kind of preparation method of 2-amino-5-chloro-N,3-dimethylbenzamide
abstract The invention relates to a preparation method of 2-amino-5-chloro-N,3-dimethylbenzamide. The preparation method comprises the following steps: taking 2-nitro-3-methylbenzoic acid as a starting material, successively undergoing reduction reaction, chlorination reaction, esterification reaction and ammonolysis reaction to obtain 2-amino-5-chloro ‑N,3‑Dimethylbenzamide. The preparation method of the present invention provides a new path for the synthesis of 2-amino-5-chloro-N, 3-dimethylbenzamide, the yield of the whole route can reach more than 80%, and the cost is significantly reduced. The reaction conditions are mild, the amount of three wastes is small, and it is suitable for industrial production.
priorityDate 2020-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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