http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111517975-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C227-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C231-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C227-16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C227-18 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C237-30 |
filingDate | 2020-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-12-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2022-12-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-111517975-B |
titleOfInvention | A kind of preparation method of 2-amino-5-chloro-N,3-dimethylbenzamide |
abstract | The invention relates to a preparation method of 2-amino-5-chloro-N,3-dimethylbenzamide. The preparation method comprises the following steps: taking 2-nitro-3-methylbenzoic acid as a starting material, successively undergoing reduction reaction, chlorination reaction, esterification reaction and ammonolysis reaction to obtain 2-amino-5-chloro ‑N,3‑Dimethylbenzamide. The preparation method of the present invention provides a new path for the synthesis of 2-amino-5-chloro-N, 3-dimethylbenzamide, the yield of the whole route can reach more than 80%, and the cost is significantly reduced. The reaction conditions are mild, the amount of three wastes is small, and it is suitable for industrial production. |
priorityDate | 2020-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 73.