http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111321179-A
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_a701be287981eecc551703d37254905a |
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C12P17-182 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C12P17-18 |
| filingDate | 2018-12-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0dc81b5356cf2b97dd431bd613e09130 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_232e70b5916456e3a6e850f7e4d150c0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2c6f9891022e49ace4dab9934a95c520 |
| publicationDate | 2020-06-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-111321179-A |
| titleOfInvention | Method for preparing matrine from subprostrate sophora |
| abstract | The invention provides a method for preparing matrine from subprostrate sophora root, which comprises the following steps: crushing the vietnamese sophora root, adding an ethanol solution, leaching for 1-3 hours at a high temperature of 80-90 ℃, and filtering to obtain filtrate I and filter residue I; adding 5-10% of an Aspergillus niger liquid chamber into the filter residue I, carrying out warm fermentation for 3-8 days, adding an ethanol solution, carrying out high-temperature leaching at 80-90 ℃ for 1-3 h, and filtering to obtain a filtrate II; mixing the filtrate I and the filtrate II, concentrating under reduced pressure, and extracting with ethyl acetate with a volume twice to four times that of the filtrate I to obtain a water phase; adjusting the pH value of the water phase to 7.5-8, and extracting with butanol with a volume which is two to four times that of the water phase to obtain a butanol phase; concentrating butanol phase, loading on ADS-7 column, eluting with ethanol solution four times to six times column volume to obtain eluate I; and concentrating the eluent I, crystallizing overnight at 4-8 ℃, and filtering to obtain a matrine product. |
| isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112174963-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112174963-B |
| priorityDate | 2018-12-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 41.