http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111303317-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08C19-02 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08C19-02 |
filingDate | 2020-04-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-04-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2022-04-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-111303317-B |
titleOfInvention | Method for preparing hydrogenated copolymer from conjugated diene hydrogenated latex |
abstract | The invention provides a method for preparing hydrogenated copolymer by conjugated diene hydrogenation latex, which comprises the following steps: mixing part of the conjugated diene rubber latex with a Holveda-Grubbs II catalyst to obtain a mixture A; mixing the residual conjugated diene rubber latex, the mixture A and a compound additive to obtain a mixture B; the composite auxiliary agent is selected from two or more of sodium oleate, potassium oleate, tetradecenyl sodium sulfonate, tetradecenyl potassium sulfonate, linear alkyl sulfate and alkyl betaine; introducing nitrogen into the mixture B to perform stirring and degassing treatment, and then continuing stirring treatment to obtain a mixture C; and (3) heating the mixture C, introducing hydrogen, and carrying out hydrogenation reaction to obtain a hydrogenated copolymer. Through a batch-adding mixing mode, specific composite auxiliaries are introduced, nitrogen is degassed and then stirred, selective hydrogenation of conjugated diene is achieved, the using amount of a catalyst is reduced, a product with a high hydrogenation degree is obtained, the reaction rate is accelerated, and the catalytic efficiency is improved. |
priorityDate | 2020-04-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 67.