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publicationDate 2020-06-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-111257439-A
titleOfInvention Determination of Hydroxypolybrominated Diphenyl Ethers in Aquatic Products by Solid Phase Extraction-Ultra Performance Liquid Chromatography Tandem Mass Spectrometry
abstract The invention relates to the technical field of detection of hydroxy polybrominated diphenyl ethers. In view of the problems that GC-MS detection of hydroxy polybrominated diphenyl ethers requires derivatization, and incomplete derivatization will lead to inaccurate quantitative results, a solid-phase extraction-ultra high performance liquid chromatography series connection is provided. The method for detecting hydroxypolybrominated diphenyl ethers in aquatic products by mass spectrometry includes the following steps: 1) extracting the aquatic products with an extractant to obtain an extract; 2) purifying the extract by solid phase extraction to remove impurities to obtain a decontamination solution; 3) removing impurities The liquid was detected by ultra-high performance liquid chromatography tandem mass spectrometry and quantified by external standard method. The method can realize quantitative and qualitative analysis of trace amount of hydroxypolybrominated diphenyl ethers in aquatic products, has the advantages of convenient operation, good reproducibility, accurate qualitative and high recovery rate, etc. Method for the determination of hydroxypolybrominated diphenyl ethers.
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