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filingDate 2019-10-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9522f7b7a6bcee6586cfeb868b6fc230
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publicationDate 2020-05-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-111138292-A
titleOfInvention Process for the manufacture of 1,1,1-trifluoro-2-chloroethane and/or trifluoroethylamine
abstract The present invention relates to a process for the production of 1,1,1-trifluoro-2-chloroethane (HCFC-133a) and/or trifluoroethylamine (TFEA), wherein at least one reaction step is in a microreactor conduct. In particular, preferred embodiments of the present invention relate to a process for the production of 1,1,1-trifluoro-2-chloroethane (HCFC-133a) and/or trifluoroethylamine (TFEA), wherein at least one of The reaction steps are carried out in microreactors constructed or fabricated from SiC ("SiC microreactors") or in microreactors constructed or fabricated from alloys such as Hastelloy C. In the manufacture of HCFC-133a and/or TFEA, HCFC-133a and/or TEFA can be readily purified and/or isolated, for example, using only low-energy-consuming methods, and the method of purification and/or isolation preferably does not require Distilled. Advantageously, HCFC-133a and/or TEFA can be easily and energy-efficiently separated from excess HF and catalyst by phase separation.
priorityDate 2018-11-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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