http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110938202-A

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filingDate 2019-12-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_86effaa60c033c329d833de051086b41
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publicationDate 2020-03-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110938202-A
titleOfInvention Preparation method of Mannich flame-retardant polyether polyol
abstract The invention belongs to the technical field of preparation of flame-retardant polyether polyol, and particularly relates to a preparation method of Mannich flame-retardant polyether polyol. The method comprises the steps of adopting an aromatic phenol compound, paraformaldehyde or a formaldehyde aqueous solution to react with diethanol amine to prepare Mannich base, reacting the Mannich base with phosphorus oxychloride to generate a chlorine and phosphorus element modified Mannich base initiator, simultaneously controlling the proportion and the feeding mode of the phosphorus oxychloride, modifying Mannich base molecules through phosphorus oxychloride groups to synthesize a macromolecular Mannich base initiator with higher functionality, and finally carrying out polymerization reaction on the macromolecular Mannich base initiator and alkane oxide to obtain the special Mannich flame-retardant polyether polyol.
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