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filingDate 2019-12-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-06-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-06-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110918126-B
titleOfInvention Preparation method of flower-shaped molybdenum disulfide combined UiO-66 photocatalyst
abstract The invention relates to a preparation method of a flower-shaped molybdenum disulfide combined UiO-66 photocatalyst, which comprises the steps of firstly, taking zirconium salt and an organic ligand as precursors, taking a polar solvent as a dispersing agent, and preparing a white solid product, namely spherical UiO-66 nano particles, by adopting a solvothermal method; then, dispersing the spherical UiO-66 nano particles in distilled water to form a milky white solution; sequentially adding a molybdenum source and a sulfur source into the milky white solution, ultrasonically dissolving and stirring for 30 min, transferring the milky white solution into a high-pressure autoclave with a polytetrafluoroethylene lining, heating at a constant temperature, cooling to room temperature, and performing centrifugal separation to obtain a gray black product; and finally, washing the grey-black product by absolute ethyl alcohol, and drying in vacuum to constant weight to obtain the flower-shaped molybdenum disulfide combined UiO-66 photocatalyst. The method has the advantages of simple operation, easily obtained raw materials and low cost, and the obtained photocatalyst has excellent photocatalytic degradation performance.
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