http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110749614-A

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filingDate 2019-11-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_48a5e904d3f04c07f586080371cb2ece
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publicationDate 2020-02-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110749614-A
titleOfInvention A method for rapid quantitative detection of organic phosphorus in soil
abstract The invention relates to a method for rapid quantitative detection of organic phosphorus in soil. A soil sample is added to a mixed solution of 0.25M NaOH and 0.05M Na 2 EDTA, extracted by shaking in the dark, and then centrifuged, the supernatant is collected and filtered, and the supernatant is collected. Clear and freeze to obtain lyophilized powder; take 50 mg of lyophilized powder, dissolve it in 2 mL of paramagnetic ion solution, vortex and let stand to obtain a liquid 31 P NMR sample, which is detected by a Bruker 600MHz liquid nuclear magnetic resonance spectrometer. The chemical shift value of the P signal can determine the organic phosphorus form corresponding to the signal, and according to the relative ratio of the signal peak intensity, the relative abundance of a certain or a certain type of organic phosphorus can be determined to calculate its content. Compared with the common liquid 31 P NMR method, the invention shortens the detection time of the NMR experiment and improves the efficiency of quantitative analysis of soil organic phosphorus.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112964774-B
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priorityDate 2019-11-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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Total number of triples: 27.