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filingDate 2019-11-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-11-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-11-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110699702-B
titleOfInvention Hillock-shaped in-situ nickel-vanadium double metal hydroxide catalyst and preparation method and application thereof
abstract The invention discloses a hill-shaped in-situ nickel-vanadium double metal hydroxide catalyst and a preparation method and application thereof, and the method comprises the following steps: pretreating foamed nickel; step two: adding vanadium chloride and urea into a mixed solvent of alcohol and N-methyl pyrrolidone; step three: soaking the foamed nickel in the solution A to perform a solvothermal reaction at 115-125 ℃ for 23-25 h; step four: after the reaction is finished, naturally cooling the reaction kettle to room temperature, alternately cleaning the reaction kettle by water and alcohol, collecting and drying the reaction kettle to obtain a hill-shaped in-situ nickel-vanadium double metal hydroxide catalyst; the method has the characteristics of simple preparation process, low synthesis temperature, no need of large-scale equipment and harsh conditions and the like by adopting a solvothermal method, and the prepared hill-shaped in-situ nickel-vanadium double metal hydroxide catalyst has high activity and high stability and has good full-hydrolytic performance under alkaline and neutral conditions.
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