http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110684989-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C25B3-00 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C25B3-00 |
filingDate | 2019-10-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2020-08-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2020-08-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-110684989-B |
titleOfInvention | Method for electrochemically synthesizing 6-azido methyl phenanthridine compound |
abstract | The invention discloses a method for electrochemically synthesizing 6-azido methyl phenanthridine compounds, and belongs to the technical field of chemical synthesis. The synthesis method of the invention uses distyryl azide and sodium azide as raw materials, uses a mixed solution of acetonitrile and water as a solvent, and directly prepares the 6-azido methyl phenanthridine compound by an electrochemical method. The method has simple synthesis steps, solves the problems of high cost and long required time of the conventional synthesis method, and has mild reaction conditions because the reaction is carried out at room temperature. In addition, the electrochemical reaction of the invention only needs to be electrified, does not need complex photochemical reaction equipment, and has low requirements on instruments and equipment. |
priorityDate | 2019-10-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 41.