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filingDate 2019-11-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-05-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-05-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110668496-B
titleOfInvention Method for preparing rutile TiO by HCl volatilization low-temperature method2Nano powder
abstract The invention discloses rutile TiO with high photocatalytic performance applicable to ultraviolet light and visible light 2 Nano powder, its preparation method by adopting HCl volatilization low-temp 2 The particle size of the nano powder is 6-23 nm. In the range of concentrated HCl with the volume ratio of water to the concentrated HCl being 80-100: 0.2-2, the HCl in the mixed solution is promoted to be continuously volatilized by prolonging the standing aging time, and the rutile TiO is promoted 2 Can realize anatase to rutile TiO after being calcined at the temperature of 200 ℃ and above 2 Thereby resulting in the formation of single-phase rutile TiO of high crystallinity 2 . TEM images show TiO calcined at 200 ℃ 2 The nano particles are bamboo leaf-shaped, porous, highly crystalline and nano-structured, show the best photocatalytic performance, the degradation rate of methyl orange after 2 hours of ultraviolet irradiation reaches 87%, and the degradation rate of methyl orange after 2 hours of visible light irradiation reaches 49.1%. Prepared rutile type TiO 2 The nano powder is suitable for photocatalysis, sensors and dye sensitizationSolar cells, and the like.
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