http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110568101-B
Outgoing Links
Predicate | Object |
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classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N2030-062 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-8631 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-72 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N30-06 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-86 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-72 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-02 |
filingDate | 2019-09-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-04-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2022-04-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-110568101-B |
titleOfInvention | Method for determining volatile and semi-volatile components in cut tobacco based on HS-SPME-GC-MS/MS |
abstract | The invention relates to a method for determining volatile and semi-volatile components in tobacco shreds based on HS-SPME-GC-MS/MS, belonging to the technical field of analytical chemistry. Taking a plurality of cigarette samples, discarding filter sticks, cutting, taking tobacco shreds, freezing at-80 ℃ for 28-32min, taking out and crushing into tobacco powder; taking naphthalene as an internal standard, weighing 0.5g of tobacco powder, putting the tobacco powder into a headspace bottle, adding 1mL of saturated sodium chloride solution, adding 30uL of acetone solution of 6 mu g/mL of naphthalene, quickly covering the bottle cap, detecting by adopting HS-SPME-GC-MS/MS, and quantifying by using an internal standard method. The method is based on HS-SPME-GC-MS/MS to measure the volatile and semi-volatile components in the cut tobacco, has simple sample pretreatment and accurate quantification, and is relatively comprehensive in analysis of the volatile and semi-volatile components in the cut tobacco, and easy to popularize and apply. |
priorityDate | 2019-09-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 181.