http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110483376-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J21-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D211-74 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D211-74 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J21-10 |
filingDate | 2019-09-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2020-11-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2020-11-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-110483376-B |
titleOfInvention | Synthesis method of intermediate N-phenyl-4-piperidone |
abstract | The invention discloses a synthetic method of an intermediate N-phenyl-4-piperidone, which comprises the following steps: dissolving aniline in ether, adding a catalyst, adding 3-methyl-1, 3, 5-pentanetriol under stirring, heating for reflux reaction, filtering after the reaction is finished, and distilling under reduced pressure to obtain N-phenyl-4-methyl-4-piperidinol; then, demethylation and oxidation reaction are carried out to prepare the N-phenyl-4-piperidone. The synthesis method has the advantages of simple preparation process operation, short production process, high raw material conversion rate, low production cost and high economic benefit. |
priorityDate | 2019-09-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 60.