http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110483364-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D209-34 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D209-34 |
| filingDate | 2019-08-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2020-12-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2020-12-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-110483364-B |
| titleOfInvention | Indolone sulfone compound and synthesis method thereof |
| abstract | The invention belongs to the technical field of organic chemistry, and particularly relates to a preparation method of indolone sulfone compounds. The structure of the compound is shown in the specification 1 H NMR、 13 C NMR, single crystal diffraction and the like. The method of the invention is that acetonitrile is used as a solvent, tetrabutyl is used for iodinationAmmonium is taken as an additive, and N- (2-iodophenyl) -N-methyl methacrylamide, a sulfur dioxide solid substitute and enol silyl ether react under the condition of ultraviolet irradiation of a mercury lamp at room temperature to obtain the indolone sulfone compound. The preparation method of the indolone sulfone compound has the advantages of mild conditions, simplicity, high efficiency, high reaction yield, wide application range of the substrate, good product purity, convenience for separation and purification and good application value. |
| priorityDate | 2019-08-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 50.