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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07J73-003
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07J73-00
filingDate 2019-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-11-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-11-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110452284-B
titleOfInvention Preparation method of 28-high brassinolide
abstract The invention relates to a preparation method of 28-high brassinolide, belonging to the technical field of organic synthesis. The invention takes (2,22) -diene-24S-ethyl-5 alpha-cholest-6-ketone as a raw material to obtain the compound through two steps of Sharpless asymmetric double hydroxylation and Baeyer-Villiger oxidation reaction under the action of a chiral catalyst and an oxidant. The method has the advantages of high efficiency, environmental friendliness, few steps, simple process, convenient operation and good industrial application value.
priorityDate 2019-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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