http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110422821-A

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filingDate 2019-07-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5797d51610384ad29fc925ebe4f87291
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publicationDate 2019-11-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110422821-A
titleOfInvention Preparation method and application of one-dimensional anatase phase TiO2 nanocone array
abstract The invention discloses a preparation method and application of a one-dimensional anatase phase TiO2 nanocone array, which comprises the following steps: (1) adding concentrated sulfuric acid and concentrated hydrochloric acid solution into ultrapure water and fully stirring to obtain the first mixed (2) When the temperature of the first mixed solution drops to room temperature, add the titanium source precursor and continue to stir to obtain a transparent mixed solution; (3) pour the transparent mixed solution into a stainless steel reactor with a polytetrafluoroethylene liner , place a piece of FTO conductive glass substrate in the inner lining of the reactor, with the conductive side of the glass facing down, put the reactor into a constant temperature drying oven for reaction, after the reaction is completed, wait for it to cool naturally to room temperature, take out the glass substrate, and place Ultrasonic cleaning was performed in a mixture of water and ethanol. This method successfully uses highly crystalline, highly oriented one-dimensional anatase phase TiO2 nanocone arrays as electron transport materials for perovskite solar cells, and achieved a conversion efficiency as high as 22.48%.
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