http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110408048-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G83-008 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C06B43-00 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C06B43-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G83-00 |
filingDate | 2019-09-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2021-06-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2021-06-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-110408048-B |
titleOfInvention | Insensitive energetic metal organic framework and preparation method thereof |
abstract | The invention discloses a silver-based cationic energetic metal organic framework and a preparation method thereof, and the preparation method comprises the following steps: step 1: commercial organic intermediate 3-amino-1H-1, 2, 4-triazole-5-carboxylic acid is used as a starting material, and concentrated H is added into anhydrous methanol 2 SO 4 The synthesis of methyl 5-amino-1H-1, 2, 4-triazole-3-carboxylate (MATC) was carried out as a catalyst; step 2: MATC is used for reacting with hydrazine hydrate to prepare target non-energetic nitrogen-rich ligand 3-amino-1H-1, 2, 4-triazole-5-carbohydrazide (ATCA); and step 3: suspending a certain amount of ATCA in hot water, heating until the ATCA is dissolved, then adding a certain concentration of silver perchlorate solution, dropwise adding a certain amount of perchloric acid, and slowly cooling, evaporating and crystallizing to obtain the target product of silver-based cationic energetic metal organic framework. |
priorityDate | 2019-09-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 62.