abstract |
The present invention relates to a kind of preparation methods that drug second poplar benzene willow amine is prepared using carbasalate calcium finished mother liquid recovery article;Recycling calcium salicylate is acted on by the oxide or hydroxide of carbasalate calcium finished mother liquid and calcium the present invention provides a kind of, calcium salicylate reacts the new preparation process for preparing Trial of Etofesalamide with 4- phenetidine under condensing agent effect again;The process stabilizing, easy to operate, with short production cycle, good product quality, high income, conversion ratio almost 100% realize comprehensive cyclic utilization, and production cost is low, and low energy consumption, and the three wastes are few, are suitble to industrialized production. |