http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110357769-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C45-676 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C49-16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C45-67 |
filingDate | 2019-08-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-08-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2022-08-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-110357769-B |
titleOfInvention | A kind of continuous flow method for preparing 3,5-dichloro-2-pentanone |
abstract | The invention relates to a continuous flow method for preparing 3,5-dichloro-2-pentanone. In a continuous flow reaction device, α-acetyl-α-chloro-γ-butyrolactone and hydrochloric acid are simultaneously mixed with a metering pump. It is pumped into the reaction device and continuously reacted at 50-90 °C to obtain 3,5-dichloro-2-pentanone. Compared with the traditional kettle type reaction method, the technical scheme of the invention avoids long-term contact between the product and the acid, the product has a short residence time, does not generate by-products and tar, and has the advantages of simple operation and post-processing, and high product yield and purity. advantage. |
priorityDate | 2019-08-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 17.