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filingDate 2019-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_fb383013d9dec59ccae2b4bf94685a19
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publicationDate 2019-09-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110256503-A
titleOfInvention A kind of preparation method of high-purity tris(dibenzylideneacetone)dipalladium(0)
abstract The invention discloses a method for preparing high-purity tris(dibenzylideneacetone)dipalladium(0). The method comprises: 1. Under a nitrogen atmosphere, the ligands dibenzylideneacetone, palladium dichloride and Anhydrous sodium acetate is added in the dehydrated alcohol of stirring state and heated reaction, obtains solid bis (dibenzylidene acetone) palladium (0) after filtering; Benzylacetone) palladium (0) was added into the stirred acetone for reaction, the retentate was washed after filtration, and the washed retentate was dried to obtain tris(dibenzylideneacetone)dipalladium(0). The present invention adopts dehydrated alcohol, dibenzylidene acetone, palladium dichloride and anhydrous sodium acetate to first prepare bis(dibenzylidene acetone) palladium (0), and then obtains tris(dibenzylidene acetone) through acetone solution treatment ) Dipalladium (0), the prepared three (dibenzylideneacetone) dipalladium (0) has higher purity.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111471073-A
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priorityDate 2019-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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