http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110256503-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_32d48279c090f590b82ea531a20ddd8d |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F15-006 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F15-00 |
filingDate | 2019-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_fb383013d9dec59ccae2b4bf94685a19 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_cb340df4531eb94a5704b973d47ee4b9 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_abecd7d26086e43ef5da161db46f774b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4dd3de3a4fcf7e3fe27be0318d1abb60 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b41ffd6796c44ecb52496692633f7347 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a4924073d1b76fa130f02fe40215c871 |
publicationDate | 2019-09-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-110256503-A |
titleOfInvention | A kind of preparation method of high-purity tris(dibenzylideneacetone)dipalladium(0) |
abstract | The invention discloses a method for preparing high-purity tris(dibenzylideneacetone)dipalladium(0). The method comprises: 1. Under a nitrogen atmosphere, the ligands dibenzylideneacetone, palladium dichloride and Anhydrous sodium acetate is added in the dehydrated alcohol of stirring state and heated reaction, obtains solid bis (dibenzylidene acetone) palladium (0) after filtering; Benzylacetone) palladium (0) was added into the stirred acetone for reaction, the retentate was washed after filtration, and the washed retentate was dried to obtain tris(dibenzylideneacetone)dipalladium(0). The present invention adopts dehydrated alcohol, dibenzylidene acetone, palladium dichloride and anhydrous sodium acetate to first prepare bis(dibenzylidene acetone) palladium (0), and then obtains tris(dibenzylidene acetone) through acetone solution treatment ) Dipalladium (0), the prepared three (dibenzylideneacetone) dipalladium (0) has higher purity. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111471073-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-111471073-B |
priorityDate | 2019-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 54.