http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110128321-B

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Predicate Object
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D209-48
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D209-48
filingDate 2019-05-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-02-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-02-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110128321-B
titleOfInvention Preparation method of low-yellowness diether diphthalimide
abstract The invention relates to a preparation method of low-yellowness diether diphthalimide, which comprises the following steps: (A) reacting diphenol with strong base in non-polar solvent to prepare diphenol; (B) performing nucleophilic reaction on the product obtained in the step A and phthalimide in a polar aprotic solvent; (C) and (B) introducing methyl chloride and/or ethyl chloride gas into the system after the reaction is finished to obtain the diether diphthalimide. The invention adopts methyl chloride and/or ethyl chloride gas to react with residual phenolic hydroxyl/phenolate end groups to generate stable alkyl, and solves the problems of yellowing color and easy oxidation yellowing of the diether diphthalimide product in the prior production technology process.
priorityDate 2019-05-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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