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filingDate 2019-05-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2020-06-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2020-06-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110102331-B
titleOfInvention High-performance oxygen evolution cobalt diselenide/nickelous tetraselenide @ NC/C composite catalyst and preparation method and application thereof
abstract The invention discloses high-performance oxygen evolution CoSe 2 /Ni 3 Se 4 The @ NC/C composite catalyst and the preparation and the application thereof; the composite catalyst is formed by loading nickel-cobalt selenide nano-particles and nitrogen-doped carbon on a carbon material; the preparation method comprises the steps of mixing a nitrogenous organic micromolecule compound, cobalt salt and nickel salt through a liquid phase, evaporating a solvent, drying, placing in a protective atmosphere for primary roasting treatment, uniformly stirring a roasted product and a carbon material in a dimethyl formamide-water mixed solution, then carrying out solvothermal reaction, and placing the solvothermal reaction product in the protective atmosphere for secondary roasting treatment to obtain the catalyst. The preparation process is simple, low in cost and beneficial to industrial production; the prepared composite catalyst is applied to a storage and conversion system of renewable energy sources such as water decomposition or metal-air secondary batteries, has the characteristics of high activity and good stability, and is relatively higher than that of commercial RuO 2 The catalyst has better comprehensive performance and shows good application prospect.
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