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filingDate 2019-04-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-11-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2021-11-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110040789-B
titleOfInvention A kind of preparation method of nickel ferrite microsphere supercapacitor electrode material
abstract The invention relates to a method for preparing a nickel ferrite microsphere supercapacitor electrode material; nickel salt and iron salt are weighed and added into deionized water to dissolve them; urea and ammonium fluoride are mixed into a solvent to keep the nickel salt , iron salt, urea, and ammonium fluoride in a molar ratio of 1:2:18~36:9~24, continue stirring to form a clear solution, then transfer to the reaction kettle, and place it in an oven for constant temperature reaction; hydrothermal After the process is finished, the reaction product is naturally cooled to room temperature; after suction filtration, precipitation, washing, and drying, hollow NiFe 2 O 4 microspheres with a diameter of 2-3 μm are finally obtained. The NiFe 2 O 4 microsphere material was fabricated into electrodes by rolling method, and it had a mass specific capacitance of 204.3 F/g at a current density of 1 A/g. The method is simple, easy to implement, green and environmentally friendly, does not require subsequent heat treatment to obtain an impurity-free NiFe 2 O 4 electrode material, reduces energy consumption processes, and is easy to industrialize production.
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