http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110015975-A

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filingDate 2019-05-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0b7e0367704bfa55d5878c45e4803e73
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publicationDate 2019-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110015975-A
titleOfInvention A kind of 2-chloro-5-nitrobenzonitrile microreaction synthesis method
abstract A 2-chloro-5-nitrobenzonitrile micro-reaction synthesis method, comprising a base, a micro-reaction device arranged on the base, and a feeding device for controlling the flow rate of materials, the micro-reaction device comprising sequentially from front to back Arrange a plurality of condensation plates and reaction plates respectively sandwiched between the two condensation plates; the condensation plates include a first plate body and a second plate body attached to the first plate body, the first plate body and the second plate body are arranged. The contact surface of the plate body is provided with a condensation channel. The condensation channel includes a liquid inlet channel, a liquid outlet channel and a plurality of condensation chambers for connecting the liquid inlet channel and the liquid outlet channel. The liquid inlet channel is connected to the bottom of the condensation chamber, and the condensate liquid It moves from bottom to top in the condensation chamber; a liquid mixing device is also arranged on the base, and the invention has the following advantages: the arrangement of the micro-reaction device can slow down the speed of the nitrification reaction; the arrangement of multiple condensation plates can accurately control the reaction temperature.
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Total number of triples: 29.