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filingDate 2019-05-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2019-07-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-110002962-A
titleOfInvention A kind of extraction method of alkyl resorcinol in wheat bran
abstract The invention belongs to the field of separation and preparation of natural functional substances, and relates to a method for extracting alkylresorcinol from wheat bran. In the present invention, dry wheat bran is selected as the raw material, and after the raw material is selected, sorted and ground, ethyl acetate is added to carry out ultrasonic extraction, the supernatant is obtained after centrifugation, and the concentrated liquid is obtained by rotary evaporation. Then use solid-phase extraction or silica gel mixing to perform separation and purification by silica gel column chromatography, and then collect the eluate for further concentration to obtain a mixed solution of different homologues of alkyl resorcinol. The high-performance liquid chromatography analysis showed that the different congeners in the alkylresorcinol product had the advantages of good separation and high purity. Compared with the existing alkyl resorcinol preparation technology, the use of silica gel column chromatography to separate and purify the naturally occurring alkyl resorcinol in wheat bran greatly reduces the complexity and danger of chemical synthesis, and Strong maneuverability.
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