http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109942554-A

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_40c3a24acafc39846109b5a181a69878
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D405-06
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A01N43-50
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A01P3-00
filingDate 2019-04-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a9ef60061fe4affc7e5841f23f56a30e
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b9441d28b14ddeffcb012403325001ad
publicationDate 2019-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109942554-A
titleOfInvention A novel heterocyclic low-toxicity and high-efficiency pesticide and its preparation method and application
abstract The invention relates to a novel heterocyclic low-toxicity and high-efficiency pesticide and a preparation method and application thereof. The preparation method of the novel heterocyclic low-toxicity and high-efficiency pesticide comprises the following steps: (1) 2-thiohydantoin, benzene After furan-2-formaldehyde, piperidine and absolute ethanol are mixed, heated to reflux temperature and reacted for 2-3 hours, water is added to terminate the reaction, filtered, and the filter residue is washed successively with isopropanol, ethanol, and water, and vacuum-dried to obtain a solid; ( 2) Dissolve the solid obtained in step (1) in methanol, add sodium methoxide and methyl iodide, heat to reflux temperature for 3-5 hours, add water to stop the reaction, filter, wash the filter residue with water, and dry in vacuo to obtain the solid, which is Heterocyclic compounds of formula I.
priorityDate 2019-04-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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