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filingDate 2019-03-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_eefaef79fa51c0b68d58ca1f9d206545
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publicationDate 2019-06-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109908871-A
titleOfInvention A kind of preparation method of magnetic Fe3O4@MIL-100 and its application
abstract The invention belongs to the technical field of chemical materials, and relates to a preparation method of magnetic Fe 3 O 4 @MIL-100(Fe), in particular to a method for in-situ one-step synthesis of Fe 3 O 4 @MIL-100(Fe) by a microwave method. The preparation method of Fe 3 O 4 @MIL-100 of the present invention comprises the following steps: (1) Fe 3 O 4 preparation; (2) Fe 3 O 4 @MIL-100 (Fe) microwave synthesis. The Fe 3 O 4 /MIL-100 prepared by the invention can be used for the adsorption and photocatalytic degradation and removal of diclofenac sodium in water, and the removal effect is over 50%, and the highest can reach over 99%. And can be reused 3 times. The time required for the microwave in-situ growth process of the method is about 30 minutes, which is significantly shorter than similar materials prepared in the prior art.
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