http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109851534-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-43 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-35 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D203-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C317-32 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C315-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D203-20 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C319-20 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-32 |
filingDate | 2017-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2021-04-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2021-04-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-109851534-B |
titleOfInvention | A kind of synthetic method of florfenicol intermediate |
abstract | The present invention relates to a method for synthesizing a florfenicol intermediate (IV), which specifically comprises the following steps: dissolving compound (II) in an organic solvent, and performing mesylation under basic conditions to obtain compound (III) ); compound (III) is ring-closed under the action of a base to obtain compound (IV); compound (IV) undergoes fluorination and ring-opening to obtain florfenicol intermediate (I). The method of the invention has novel design, mild conditions, simple and convenient operation, and is suitable for industrial production. |
priorityDate | 2017-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 79.