http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109775714-A

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_55597b63b017897d85062f773c255c7a
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B33-18
filingDate 2019-01-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5a110c4e1fc9425c2ee4511dfaec98b2
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e6af4d468ac1d5dc4927cc14d64859b4
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publicationDate 2019-05-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-109775714-A
titleOfInvention A kind of MFI topology structure silicon molecular sieve containing trace rare earth ions and preparation method thereof
abstract The invention relates to the field of silicon molecular sieves, and discloses an MFI topology silicon molecular sieve containing trace rare earth ions and a preparation method thereof. The silicon molecular sieve has a BET specific surface area of 400-500 m 2 /g and a particle size of 0.15-0.25 microns , the mass ratio of silicon dioxide to rare earth ions is (10000-200000): 1, and the preparation method includes: a, mixing a silicon source, a rare earth ion source, an organic template agent and water to obtain a colloidal mixture; b, mixing step a The colloidal mixture obtained in the two-stage variable temperature hydrothermal crystallization. By adopting the method of the invention, a near-neutral silicon molecular sieve with high crystallinity, fine particles and extremely small amount of rare earth metal ions can be obtained, and the content of rare earth ions is in the range of 5-100ppm. The conversion rate of cyclohexanone oxime can prolong the life of the catalyst and improve the economy of the new process technology of gas phase rearrangement.
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type http://data.epo.org/linked-data/def/patent/Publication

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